Picture of Softmatter-Rheometer
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WARNING
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The Kinexus Prime ultra+ rotational rheometer measures shear viscosity with a parallel plate design where the sample is loaded between the plates at a known gap. The rheometer works in controlled stress or controlled rate mode. The type of measuring system used and its dimensions depend on the sample type and its viscosity. A cone-plate measuring system is typically preferred since the shear rate is constant across the sample. A measuring system with a larger surface area such as a double gap concentric cylinder is used for measuring large particle suspensions, with low viscosity.

Capabilities/Accessories

Key Parameters:

  • Torque range: 0.5 nNm to 250 mNm
  • Normal force range: 0.001N to 50N
  • Angular velocity range: 1nrad/s to 500rad/s
  • Oscillation frequency range: 1µHz to 150Hz

Measuring Geometries:

  • Plate–Plate Geometry

Interchangeable lower plate pedestal with a 61 mm diameter. Suitable for optimized thermal properties, mechanical alignment, and release mechanism.

  • Cone–Plate Geometry

Upper measuring cone with 4° opening angle and 40 mm diameter.

A gemometry with 1° opening angle and 20 mm diameter.

The geometry is optimized with respect to compliance, inertia and thermal properties.

  • Concentric cylinder (Couette Geometry)

Double-gap cylindrical geometry (C25). The system comprises an upper double-gap bob (25 mm outer diameter) and a lower stainless-steel double-gap cup, suitable for low-viscosity and complex fluids.

  • Plate Peltier Temperature Control modules.

Plate-plate and cone–plate geometries are compatible with controlled measurements over a temperature range of –40 °C to 150 °C. The concentric cylinder is compatible with a range of -25 °C to 150 °C

Tool name:
Softmatter-Rheometer
Area/room:
TA room II (C419)
Category:
Soft Matter
Manufacturer:
Netzsch
Model:
Netzsch rSpace

Rheometer Netzsch

Please read and follow these instructions before operating the rheometer. 1. COMPRESSED AIR FAILURE / POWER OUTAGE — DO NOT TOUCH THE INSTRUMENT In the event of a power outage or failure/loss of the building’s compressed-air supply: • DO NOT touch the drive spindle, geometry, or any other moving/mechanical parts. • If an experiment is ongoing when the pressure or power failure occurs, DO NOT under any circumstances attempt to remove, adjust, or move the geometry. • Do not attempt to restart or operate the instrument yourself. • The instrument MUST be inspected by the Facility Manager (Jing Li) after the full compressed-air pressure has been restored and before further use. The rheometer was previously affected by a compressed-air pressure outage on 29 July 2026 at 16:00. Extra caution is therefore required to prevent damage to the instrument and its sensitive components. 2. AIR-BEARING PROTECTION COVER When the instrument is powered OFF: • The air-bearing protection cover MUST be installed. • Remove the protection cover BEFORE switching the instrument ON. • After the instrument has been powered OFF, replace the protection cover immediately. Never operate the instrument with the protection cover installed. 3. GEOMETRY COMPATIBILITY MESSAGE When using the CP1/20 cone-and-plate geometry, a message regarding geometry compatibility may appear. If this is the expected compatibility message for the CP1/20 geometry: Press “Ignore” to proceed. If you are unsure whether the message is expected, STOP and contact Jing Li before continuing. 4. STICKY, DIFFICULT-TO-REMOVE OR HIGH-RISK SAMPLES Measurements involving highly sticky, adhesive, hard-to-remove, or otherwise potentially problematic materials must be carefully assessed BEFORE the measurement is started. Examples include, but are not limited to, sticky lignin gels and similar materials. Users MUST: • Inform Jing Li in advance about the properties of the sample. • Discuss the planned measurement and appropriate geometry/setup before using the instrument. • Follow the recommended measurement procedure and safety precautions. • Use disposable plates/geometries where required and purchase them for their own measurements when appropriate. Do NOT proceed with a potentially problematic sample without prior approval/discussion with Jing Li. 5. UNAUTHORIZED USE IS STRICTLY FORBIDDEN UNAUTHORIZED USE OF THE RHEOMETER IS STRICTLY FORBIDDEN. Users may only operate the instrument after receiving the required training and authorization. Do not allow another person to use the instrument under your booking or account unless explicitly authorized. If you are uncertain about any operation, sample, geometry, instrument status, warning message, or abnormal behaviour: STOP THE MEASUREMENT AND CONTACT JING LI. Do not attempt to troubleshoot, repair, or manipulate the instrument yourself. 6. RESPONSIBILITY FOR DAMAGE The rheometer and its geometries are sensitive and expensive equipment. Incorrect operation, unauthorized use, failure to follow these safety instructions, or negligent handling may result in serious damage. Users may be held responsible for damage to the instrument, geometries, accessories, or other equipment resulting from unauthorized use, negligence, or failure to follow the applicable instructions and safety procedures. WHEN IN DOUBT — STOP AND ASK BEFORE YOU OPERATE.

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